书名：有机化学实验（英汉双语版）ISBN：5定价：48作者：薛思佳,李萍版次：1出版时间：-08-31本书是科学出版社普通高等教育“十二五”规划教材“有机化学(第二版)立体化教材”的《有机化学实验(英汉双语版，第三版)》部分，与《有机化学(第二版)》和《有机化学学习指导(第二版)》配套出版，方便教学选用。本书采用英汉两种语言，英文为主，中文相应对照，结合国内外有机化学实验教学的实际编写而成。全书分为6章：有机化学实验的一般知识、有机化学实验的基本操作、有机化合物的制备、综合性实验、文献实验和附录。附录编写了常用实验数据、与化学和有机化学有关的Internet网址及有机化学实验操作考试复习题。Contents第三版前言第二版前言**版前言Chapter1Introduction11.1GeneralRulesfortheOrganicChemistryLab11.2GeneralLabSafety21.3DisposalofLabWaste31.4CommonLabEquipmentandApparatus41.5DryingandDryingAgent.6HeatingandCooling.7ExperimentalRecordandLaboratoryReport.8ChemicalLiterature16Chapter2BasicExperimentalTechniques.1MeltingPointDetermination.2Recrystallization.3SimpleDistillationandFractionalDistillation.4SteamDistillation.5VacuumDistillation.6SolventExtractionandSolutionWashing.7Sublimation.8RefractiveIndexDeterminationofLiquidOrganicCompound.9OpticalRotationDetermination.10ChromatographicTechniques.11SpectroscopicIdentificationofOrganicCompound63Chapter3Experiments.1PreparationofCyclohexene.2Preparationof1-Bromobutane.3PreparationofTriphenylmethanol.4PreparationofDibutylEther.5PreparationofBenzoicAcidandPhenylmethanol.6PreparationofCyclohexanone.7PreparationofHexanedioicAcid.8PreparationandCharacterizationofCinnamicAcid.9PreparationofAcetylsalicylicAcid.10Preparationofn-ButylAcetate.11Preparationofn-DibutylPhthalate.12PreparationofAcetanilide.13Preparationof4-Nitroaniline.14IsolationofCaffeineFromTeaLeaves.15Preparationof2-Furanmethanoland2-FurancarboxylicAcid.16Preparationof8-Quinolinol.17PreparationofAcetylferrocene.18BiologicalSynthesisofEthanolChapter4All-aroundExperiments.1SynthesisandCharacterizationofEthylAcetateandEthylAcetoacetate.2SynthesisofSulfanilicAcidandMethylOrange.3ExtractionandSeparationSpinachLeafPigments.4Extraction,SeparationandIdentificationCapsanthinandβ-Carotene.5CoenzymePreparationandCharacterizationofBenzoin.6PreparationandCharacterizationofBenzilicAcid.7Microwave-AssistedPreparationandCharacterizationof2-SubstitutedphenylBenzoxazoleChapter5ExperimentsfromLiterature5.1AMicroscaleSynthesisoftheDiastereomersof2,3-DibromosuccinicAcid5.2AGrignard-likeOrganicReactioninWater.3AnEfficientMicroscaleProcedurefortheSynthesisofAspirin.4ASolvent-FreeClaisenCondensationReaction.5ThePreparationofaFluorescentDye:AMicroscaleTLCExperiment.6MicrowaveMicroscaleExperiment:2-NaphthylAcetatefrom2-NaphtholChapter6Appendix.1ListoftheElementwithTheirSymbolsandAtomicMasses.2MainFamiliesofOrganicCompounds目录第1章有机化学实验的一般知识.1有机化学实验的基本规则.2有机化学实验的一般安全知识.3有机化学实验废物的处置.4常用的玻璃仪器和实验装置.5干燥与干燥剂.6加热与冷却.7实验记录和实验报告.8有机化学的文献资料第2章有机化学实验的基本操作.1熔点的测定.2重结晶.3蒸馏与分馏.4水蒸气蒸馏.5减压蒸馏.6萃取与洗涤.7升华.8液体有机化合物折光率的测定.9旋光度的测定.10色谱技术.11有机化合物的光谱鉴定第3章有机化合物的制备1.1环己烯的制备1.21-溴丁烷的制备.3三苯甲醇的制备1.4正丁醚的制备.5苯甲酸和苯甲醇的制备1.6环己酮的制备.7己二酸的制备.8肉桂酸的制备及结构表征1.9乙酰水杨酸(阿司匹林)的制备.10乙酸正丁酯的制备.11邻苯二甲酸二正丁酯的制备.12乙酰苯胺的制备.-硝基苯胺的制备.14从茶叶中提取咖啡因.15呋喃甲醇和呋喃甲酸的制备.-羟基喹啉的制备.17乙酰二茂铁的制备.18生物法合成乙醇第4章综合性实验.1乙酸乙酯和乙酰乙酸乙酯的制备和结构表征.2对氨基苯磺酸和甲基橙的制备.3从菠菜叶中提取和分离叶色素.4从红辣椒中提取、分离和鉴定辣椒红素和β-胡萝卜素.5辅酶催化安息香的制备及结构表征.6二苯基乙醇酸的制备及结构表征.72-取代苯基苯并唑的微波法合成第5章文献实验.1非对映体的2,3-二溴琥珀酸的微量合成.2在水相中进行的类似Grignard反应.3微量法合成阿司匹林.4无溶剂的Claisen缩合反应.5一种荧光染料的制备：微量TLC实验.6微波法微量实验：2-萘酚制备乙酸-2-萘酯第6章附录.1与化学有关的网址.2有机化学实验操作考试复习题